By Aris Doelman, Annie R. Gregges, Edward M. Barrall II (auth.), Roger S. Porter, Julian F. Johnson (eds.)
Thermal research cuts a extensive swathe via modern technology. inside this area, advances in instrumentation let the appliance of quantitative calorimetry to the total spectrum of contemporary fabrics. this is often illustrated might be no greater than by means of the set of contributions which make up this quantity four of Analytical Calorimetry. The examine supported during this fourth quantity of Analytical Calorimetry covers a wide selection of subject matters. the variety exhibits the sophistication which thermal research is attaining and extra ly the ever-widening purposes which are being constructed. The contributions to the amount characterize, partially, papers awarded ahead of the department of Analytical Chemistry on the Fourth Symposium on Analytical Chemistry held on the 172nd nationwide assembly of the yank Chemical Society, August 29 - September three, 1976. a number of extra key contributions are incorporated through trendy staff within the box. Julian F. Johnson Roger S. Porter v Quantitative Scanning Calorimetry with automatic information Acquisition and relief . . . . . . . 1 Aris Doelman, Annie R. Gregges, and Edward M. Barrall, II Thermodynamic houses of a chain of P-N-Alkyl-P'-Cyanobiphenyls 19 E. M. Barrall II, R. J. Cox, A. Doelman, N. Clecak, J. A. Logan, and A. R. Gregges Thermodynamic homes of a chain of 37 P-N-Alkoxy-P'-Cyanobiphenyls R. J. Cox, E. M. Barrall II, A. Doelman, N. J. Clecak, J. A. Logan, R. D. Diller, and A. R. Gregges a brand new Equation for Predicting Polyethylene Lifetimes from Thermal information fifty one Cary F.
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Additional info for Analytical Calorimetry: Volume 4
This four entropy unit (cal/mole/oK) offset is probably due to an increase in molecular dipole interactions caused by the alkoxy-bipheny1 linkage, which is supported by the thermal properties of p-n-a1ky1-p'- cyanobipheny1s. INTRODUCTION The p-n-a1ky1-p'-cyanobipheny1s along with the p-n-a1koxy materials are extremely important for the construction of smectic-type liquid crystal display panels (4,5). The inertness of the biphenyl bridge and the importance of the aromatic cyano group for the preparation of a chemically stable yet reasonably dipolar smectogenic and nematogenic liquid crystal has been *Part XLIII of a series on Order and Flow in Liquid Crystals.
If the intercalation of the solid and the interpenetration of the smectic mesophase can be verified by X-ray diffraction, then the p-n-alkyl-p'-cyanobiphenyls will be the first series of liquid crystals in which the smectic mesophase can be defined in terms of the solid phase. CONCLUSIONS The p-n-alkyl-p'-cyanobiphenyls form a consistant series of liquid crystal forming materials. Both the absolute entropy of solid+mesophase transition and the increment per methylene group correspond to the n-alkanes.
I 340 DSC Scan of p-n-Undecyl-p'-cyanobiphenyl SOK/min Heating I (I)
Analytical Calorimetry: Volume 4 by Aris Doelman, Annie R. Gregges, Edward M. Barrall II (auth.), Roger S. Porter, Julian F. Johnson (eds.)